HTR Compact

Automation Overview Laboratory Automation and Robotics Anton Paar offers more than 170 analytical solutions and is the market leader in digital density measurement and rheology. Based on 50 years of experience in laboratory instrumentation Anton Paar has taken a step forward to laboratory automation. Anton Paar’s automation solutions optimize automated workflows which address today’s key topics, namely productivity, reproducibility, and precision. A broad automation portfolio including standard products as well as fully customized solutions addresses a wide range of automation tasks reaching from high-throughput automated rheometry to sample processing and fully automated quality control for beverages. As the only provider of both lab instruments and automation, Anton Paar is perfectly set to deliver outstanding performance for sensitive automated measurement tasks in industries and applications as diverse as petrochemistry, personal care products, food, and beverages. Furthermore, Anton Paar’s global sales and service network of subsidiaries is close to you from the project definition to execution and commissioning and offers comprehensive training, support, and tailor-made maintenance and service. Automated solutions from Anton Paar represent trustworthy measuring technology and automation from a single source – where precision meets performance. HTX platform Fully customizable laboratory automation solution Alab 5000 Fully automated quality control lab for beverages directly at the filling line HTR compact High Throughput Rheometer autosampler for Anton Paar rheometers MCR 102 and MCR 302 HTR Rheometer automation for high sample throughput and complex sample handling and conditioning Modular sample processor Automatic dosing, blending, subsampling, and transferring of liquids Precision meets performance Automated high-throughput rheometers HTR compact High-throughput operation - 36 samples in two trays with 18 cups each - Sample drawer to add vials during operation - Rheometer and sample stage operate in parallel Perfectly safe and accurate workflow - Achieve lab accuracy due to mechanical decoupling of the rheometer and automation unit - Easy sample management by using job lists - LIMS integration (file transfer, database, Ethernet) - Priority samples can be introduced at any time - Four-stage programmable cleaning station (rinse, brush, clean, dry) - Beaker gripper operates with controlled force - Controlled halt upon emergency stop The HTR compact series offers automated sample handling and conditioning for rheological measurements with Anton Paar’s MCR 102 or MCR 302 rheometers in a lightweight benchtop design. It is the ideal choice for first-level rheology automation. Specifications Dimensions (W x D x H): 1570 mm x 803 mm x 1164 mm Weight (net): 300 kg Mains supply: 230V, 16A, 50/60Hz Media interfaces: compressed air, cleaning solvents Waste disposal: drain for liquids Communication interface: Ethernet MCR 102MCR 302 Unit Max. torque 200200 mNm Min. torque, rotation 51 nNm Min. torque, oscillation 7.50.5 nNm Max. angular velocity 314314 rad/s Max. angular frequency 628628 rad/s Normal force range 0.01 to 500.005 to 50 N Rheometer specificationsOptional modules - Capping/decapping of sample vials - Different types of sample racks - Bar code reader for sample identification - Wide range of measurement geometries available from CC10 to CC27 including third-party T-bars and stirrers - Ventilation for volatile and solvent-based samples Automated high-throughput rheometers HTR Maximized operation flexibility - Up to 96 measuring geometry units (e.g. for polymer melts) - 3 different rheological geometries (CC, CP, PP) - Standard rack configuration holds 96 samples - Different types of racks for pipettes, syringes, and trim blades - Temperature-controlled sample storage (down to 4 °C) Perfectly safe and accurate workflow - Achieves lab accuracy due to mechanical decoupling of rheometer and automation unit - Sample management by using job lists - LIMS integration (file transfer, database, Ethernet) - Priority samples can be introduced at any time - Four-stage programmable cleaning station (rinse, brush, clean, dry) - Integrated trim tool removes excessive sample material to avoid wrong measurement results - Visual verification of trim result The HTR automation series offers an optimized analysis workflow for rheological investigations based on Anton Paar’s MCR 702 rheometer. The extensive set of features and the built-in flexibility make it the ideal choice for sophisticated and high-throughput R&D or QC work. Specifications Dimensions (W x D x H): 1800 mm x 1200 mm x 2000 mm Weight: 900 kg Mains supply: 400 VAC, 16A, 50/60 Hz Media interfaces: compressed air, cleaning solvents Waste disposal: drain for liquids Communication interface: Ethernet MCR 702 MultiDriveUnit Max. torque 230mNm Min. torque, rotation 1nNm Min. torque, oscillation 0.5nNm Max. angular velocity 314rad/s Max. angular frequency 628rad/s Normal force range 0.005 to 50N Rheometer specificationsOptional modules - Gravimetric and volumetric dosing and weighing - pH measurement - Capping/decapping of sample cups or vials - Various gripper tools for samples, measurement geometries, and disposables - Precise dosing of sample liquids via pipettes and/ or syringes - Automatic cutting of pipette opening to reduce shear stress - Shaker module for reproducible shaking - Barcode reader for sample identification, process control, and logging - Ventilation for volatile and solvent-based samples Automated handling of liquids and powders Modular Sample Processor Process liquids, pastes, and powder - Viscosities up to 1000 mPa.s - Input volumes from a few µL up to 1 liter - Powder samples upon request Perfectly dilute, dispense, add, and blend - Gravimetrically controlled sample volume - Accuracy of +/-0.9 mg - Drip protection avoids contamination of vials Seamlessly identify and process samples - ID-tag-based workflow programming - ID-tag-based process log file - Multiple ID tag formats: bar code, data matrix, QR - Sample management by using job lists - LIMS integration (file transfer, database, Ethernet) - Priority samples can be introduced at any time The Modular Sample Processor carries out automatic dosing, blending, subsampling, and transferring of liquids prior to analysis. It is available as a stand-alone benchtop unit or can optionally be inte\ grated into complete automated workflows. With individual adaptations the Modular Sample Processor perfectly carries out any desired liquid handling operation. Specifications Dimensions (W x D x H): 1545 mm x 803 mm x 1164 mm Weight: 180 kg Mains supply: 230 V, 16A, 50/60 Hz Communication interface: Ethernet Media interfaces: liquids for dilution, compressed air Optional modules - pH measurement module - Capping/decapping of sample vials - Various gripper tools - Automatic cutting of pipette opening to reduce shear stress - Shaker module for reproducible shaking - Different types of racks and accessories Open to customer-specific adaptations - Design and interfaces adaptable to fit into existing lab workflows - Fully customizable design upon request For customized laboratory workflows HTX automation platform Assemble individual workflows - Instruments include viscometers, density meters, refractometers, polarimeters, rheometers, etc. - Optional third-party analyzers include heating ovens, analyzers with flow cells, balances, etc. - Can be configured as a large-capacity sample processor and/or analyzer - Ten slots available for any combination of lab instruments and/or sample racks - Sample preparation and analyzers work independently of each other - Multiparameter analysis within one workflow - Redundant module configuration minimizes downtime in case of maintenance For optional modules please see the overview table. Simplify process control - Intuitive, simple-to-use control software for sample and workflow management - Sample management by using job lists - Priority samples can be introduced at any time - Broad variety of notification services (e.g. text messages or email) Communicate safely - Standard industry protocols such as PROFINET, Ethernet, CANOpen, or Profibus - LIMS integration (file transfer, database, Ethernet) The HTX floor-standing automation platform can integrate up to ten different analytical instruments such as viscometers, density meters, or refractometers for concurrent multi-parameter analysis. Its modular concept allows fully customized workflows for sample conditioning, preparation, and measurement. Specifications Dimensions (W x D x H): 2760 mm x 1600 mm x 2560 mm Weight: 800 kg net weight 1200 kg with 6 modules Mains supply: 400VAC, 16A, 50/60Hz 11 kW with 6 modules Media interfaces: 3x solvent (toluene, ethanol, isopropanol), compressed air Waste disposal: drain for liquids, waste bin for solids, ventilation for fumes Communication interface: Ethernet HTV – High Throughput Viscometer - State-of-the-art replacement of outdated Houillon viscometers based on the HTX platform - Significantly higher accuracy - High dynamic range with single measuring cell - Processes up to 2500 samples per day - Ready-made configuration based on HTX platform - Equipped with up to six SVM-type viscometers - Up to four sample racks with 96 vials - Complies to ASTM D7042 standard - Fully automatic cleaning of measuring cell - Automatic, periodic re-calibration with standard oils - Particle Quantification Index integration possible upon request - Applications: used oils, lube oils, fuels, chemicals, cosmetics Automated QC of beverages directly at the line Alab 5000 Perfectly reproducible results - Integrated air conditioning to provide a lab environment - Automatic shaker functionality ensures reproducible equilibration of the sample - Direct measurement of many different types of packages with the piercing module - Automated data acquisition and documentation Rely on production within specifications - Proven high-accuracy Anton Paar packaged beverage analyzing systems (PBA) determining CO 2, O 2, density, °Brix, alcohol, sugar inversion, TPO, and pH) - Monitors key package parameters such as torque and net content - Continuous reference measurements to monitor, adjust, and calibrate the process equipment - Seamless integration into Anton Paar’s Davis 5 software solution Alab 5000 is a fully automated quality control lab which continuously measures all key parameters of beers, soft drinks, and mineral water right after the final filling. \ It consists of four modules: one for piercing and shaking, one for the beverage analysis, one for weighing in order to determine the net content, and a torque module to measure the opening torque and the application angle. Its modular design and small dimensions make it a perfect fit for both n\ ew installations and existing production lines. Alab 5000 can also be seamlessly used with Anton Paar’\ s Davis 5 software solution supporting real-time control of the complete production process. Specifications Dimensions (W x D x H): 730 mm x 940 mm x 2270 mm One module Weight: 180 kg Mains supply: 400VAC, 32A, 50/60Hz Media interface: cleaning solvents, compressed air Waste disposal: drain for liquids, waste bin for packages Communication interface: Ethernet Adapt system configuration to actual needs - Flexible design comprising four individual modules - Small dimensions of modules enable easy transportation and installation in existing facilities - Perfectly fits into existing conveyor belt layouts requiring minimum extra space - Distributed placement of individual modules along production lines (e.g. delayed torque measurement) Available configurations - Standard setup includes analytical and pierce and shake modules - Torque and weighing modules - Other measurement parameters upon request Reference projects SubjectWear monitoring of used oil samples Subsampling of urine specimens for drug testing Chemical testing of rubber specimensInline quality control of beverages Customer A global player in petrochemistry A governmental drug testing lab A leading global producer of tiresA global player in the beverage industry Samples Used oil/crude oil Biohazardous organic samples Rubber samplesSoft drinks Solution HTV High Throughput Viscometer Tailor-made automation solution based on Modular Sample Processor Tailor-made automation solution based on Modular Sample Processor Alab 5000 Automated beverage lab Modules Six SVM modules, two sample trays, two PQI modules, LIMS interface Sample drawers, capper, shaker, syringe dispenser, weighing unit, video surveillance, sample racks Sample rack, capper, gravimetric dosing unit, filter handling, waste disposal, dilution unit Pierce and shake module, analytical box, weighing and torque Challenge Replace formerly used Houillon viscometers with a more precise, state-of-the-art SVM viscometer which also represents the new standard in used oil testing; optimize cleaning procedures and measurement cycle time Provide traceable subsamples without human interaction and risk of manipulation (tamperproof); integration of subsampling station into a fully automated drug testing laboratory Handling of highly flammable solvents and risk assessment of the overall solution; fully automatic utilization of disposable filter eleme\ nts Rugged design to withstand typical production environments of bottling facilities with CIP/SIP cycles Subject Rheological testing of plant material Rheological investigation of polymer melts in R&D Goods-in quality control of coatingsIn-process product quality control Customer A start-up R&D and production plant for vegan food A leading polymer supplier in the Middle East A leading global supplier of automotive componentsA multinational producer of cosmetics and toiletries Samples Preconditioned plant material Various types of polymer melts Water-based paint and varnishToothpaste Solution HTR High Throughput Rheometer HTR High Throughput Rheometer HTR compactHTR compact Modules MCR 502 rheometer, capper/decapper, cleaning unit, pipette handler, cooled sample storage, solvent trap, trim tool MCR 502 rheometer, vacuum gripper, sample storage, measurement systems storage, trim tool Standard configuration, sample racks, temperature units Customized configuration, sample drawer, infrared temperature measurement, T-bar as stirrer Challenge Optimize workflow to avoid shear stress during sample treatment potentially resulting in compromised sample properties Optimize workflow in order to avoid system contamination due to stringing of the melted polymer sample after the measurement Design and implement intuitive and simple GUI in order to significantly reduce new operator training period at times of high operator fluctuation rate Utilization of customer beakers and stirrer instead of Anton Paar standard; develop robust detection method to ensure consistent start conditions according to customer SOP CONCEPTION PHASE IMPLEMENTATION PHASE Making complex workflows run well There is nothing available off-the-shelf which meets your 852UA#?Dv?F? ?S?@T??1AU?r??!`BvYP ? automation solutions in one go for all industry segments. With its expertise in-house Anton Paar can either customize an existing automation system or design a completely new automated workflow based on your specific requirements. How ideas take shape You can rely on one single competent partner throughout the whole life cycle of your tailor-made automation solution. Anton Paar offers modular solutions which allow you to stay flexible and adapt your system to future requirements. Together with you, Anton Paar develops the most beneficial automation solution for your workflow, from the first idea up to the final implementation at your facility. Tailor-made automation – solutions made for you ANALYTICAL WORKFLOW ASSESSMENT Investigation of the analytical workflows, mapping of status quo, recommendation of automation technology. SYSTEM CONFIGURATION Delivery of a cost and time estimate based on the draft system for further optimization. REQUIREMENT SPECIFICATIONS Specification of workflow and process performance (throughput, capacity, tolerance levels, operation conditions, etc.). QUOTE ISSUING AND CONTRACT SIGNING Once both parties agree on the final specifications and conditions, a binding quotation is issued. 1 2 3 4 SYSTEM DESIGN AND MANUFACTURING The components are manufactured or procured and the complete system is assembled, tested, and documented. SITE ACCEPTANCE TESTS The system is delivered, installed, tested (operational), and operators are trained. FACTORY ACCEPTANCE TESTS Your staff verifies the system performance at Anton Paar and receives initial training. LIFE CYCLE MANAGEMENT Execution of the maintenance contract guarantees that your system performs properly throughout its lifetime. 5 6 7 8 HTR compactHTRModular Sample Processor HTX Alab 5000 Rheometer autosampler for high sample throughput Rheometer automation for high sample throughput and complex sample handling and conditioning Modular sample processor for automatic dosing, blending, subsampling, transferring of liquids Measurement of viscosity, density, concentration of liquids, automated and expandable for other parameters Automated beverage analysis directly at the filling line Gravimetric & volumetric dosing and weighing Precise sampling and diluting of samples; gravimetric control and calculation of the sampled volume; the value is used for subsequent analysis. Used for liquids with\ low to medium viscosity. BX4?3 ??"q??"q??"qBX4?3 Filling and cleaning (flow cell) Programmable filling and cleaning cycles for analytical instruments equipp\ ed with a flow cell. Usable for all kinds of liquid solutions (inorganic and organic). BX4?3 BX4?3BX4?3??"qBX4?3 Four-stage cleaning station Cleaning in four steps which are individually programmable. Cleaning with organic solvents and/or water, brushing and drying with hot air. % A???"q* ??"q BX4?3??"qBX4?3 pH measurement Integrated pH measurement to detect the pH in addition to analytical determinations from exactly the same sample. Equipped with automatic 3-point calibration, cleaning r\ outine, and resting position. BX4?3 ??"q??"q??"qBX4?3 Capping/decapping Automatic closing and opening of each sample vial. ??"q??"q??"q??"qBX4?3 Gripper Different gripper tools are available depending on your sample containers and for pipettes. The grippers detect if the sample container or pipette is lost or cracked du\ ring transfer. BX4?3 % A???"q* ??"q ??"qBX4?3 Dispensing Precise dosing of sample liquids via pipettes and/or syringes. BX4?3??"q??"q??"qBX4?3 Pipette cutting Depending on the type of sample the pipette opening is cut to the required extent; defined via the software. BX4?3 ??"q??"q??"qBX4?3 Piercing Piercing of PET bottles, glass bottles, cans. BX4?3BX4?3BX4?3??"q % A???"q* Shaking Reproducible shaking of samples before sampling and analysis. BX4?3??"q??"q??"q % A???"q* Sample cooling station Cooling of samples down to 4 °C to avoid changes in sample properties, especially for sensitive samples and samples with volatile components. BX4?3 ??"qBX4?3??"qBX4?3 Sample racks Different types and sizes of sample racks are available. Customization of racks due to individual needs is possible on request. % A???"q* % A???"q* ??"q ??"qBX4?3 Disposable racks Different racks for pipettes, syringes, caps, trim blades are available. BX4?3??"q??"q??"qBX4?3 Measurement accessories rack Different types of racks with measurement accessories (e.g. rheological geometries) are available to support even measurements with samples which are not cleanable. BX4?3 % A???"q* BX4?3 ??"qBX4?3 Sample identification (bar code/Data Matrix/QR) For overall tracking of the sample and individual sample treatment within the workflow. ??"q??"q??"q??"q??"q * included as standard Automation functionalities document number © 2017 Anton Paar GmbH | All rights reserved. Specifications subject to change without notice. www.anton-paar.com © 2019 Anton Paar GmbH | All rights reserved. Specifications subject to change without notice. XARIP001EN_E