AutoFlow BET+

Catalysts Ceramics Energy Carbon Pharma Instrument appearance and colors subject to change. AutoFlow BET+ surface area analyzer High Throughput Surface Area Analyzer Dynamic Flow System 2 Dynamic Flow BET Analysis Visit www.quantachrome.com for more detailed instrument specifications and downloadable brochures. Achieving Highest Throughput via Modular Design High throughput matching your analytical needs is achieved with one, two or three independent analysis stations. Each Auto Flow BET+ analysis station provides highly accurate data by the implementation of: (a) two built-in mass flow controllers, making the use of premixed gases unnecessary; (b) a high-resolu- tion MEMS-TCD sensor developed by Quantachrome Instruments; and (c) precisely defined operating protocols. The AutoFlow BET+ references all mea- surements to standard temperature and pressure (STP) conditions, thereby making them calibration-free and independent of ambient conditions. The design of the instrument and its control software makes the operation very robust and user-friendly, making it ideal for both QA and academic lab applications. Assuring Extremely Rapid Surface Area Evaluations The Auto Flow BET+ can perform a typical 3-point BET measurement in less than 15 minutes per analysis station. Up to three independent analysis stations can be operated simultaneously for high throughput. The Auto Flow BET+ incorporates three different flow paths in order to optimize the analysis speed and resolution of samples covering an extremely wide range of surface areas. The Auto Flow BET+ also incorporates a 3-station sample preparation module where three samples can be degassed under dry gas flow independently and simultaneously with analyses, using multi-step user-programmable temperature ramp-and-hold protocols for each sample. Accelerating the Pace of Dynamic Flow BET Analysis The Auto Flow BET+ is a state-of-the-art dynamic flow system designed to enable an extremely rapid evaluation of the surface areas of solid samples. Single-point or multi-point determination of surface areas using different standard methods (such as BET and STSA) is easily carried out without the need for measuring system void volumes or recalibrating signal responses. Figure 1. Auto Flow BET+ with One Modular Analysis Station. Figure 2. Auto Flow BET+ with Three Modular Analysis Stations. AutoFlow BET+ surface area analyzer 3 Features Exceptional Speed • Single point BET surface areas in < 5 minutes per sample. • Multi-point BET areas in < 15 minutes per sample. • Advanced design eliminates need for pre- or post-calibration. Superior Throughput • Up to three single point BET areas in < 5 minutes. • Up to three multi-point BET areas in < 15 minutes. • Up to 36 BET surface area analyses per hour. Outstanding Precision • Repeatability (same sample) +/- 1.0% • Reproducibility (different units) +/- 3.0% • Accuracy (vs. vacuum volumetric standard) +/- 3.0% Simple Operation • Highly intuitive click-and-start operation. • No warm-up delay (ready to go when you are). • Customized analysis reports generated automatically. Accurately Pre-Calibrated • Saves analysis time (avoids calibration step). • Improves analytical precision (eliminates operator variability). • Saves cost (no need for syringes or loops). Maximum Versatility • Each module has two built-in mass flow controllers. • Modules can handle pure gases or mixed gas inputs. • Each module has an independent MEMS-TCD sensor. Robust and Reliable Design • Compact size (as little as 16-inch bench width needed). • MEMS-TCD Sensors unaffected by flow interruptions . • Virtually maintenance-free. Built-in Sample Preparation • 3 independently programmable degassers. • Adjustable flows and fast-cooling slots. • Standard max. temp. = 350 oC 450 oC with quartz sample cells (not included). Unique Software Capabilities • Supports 21 CFR Part 11 compliance. • Ethernet and Remote Access. • Multiple Language Options. AutoFlow BET+ surface area analyzer 4 Typical Applications Material(s)Standard Method(s) Metal Powders ASTM B900 Alumina, Silica A S TM C10 69 Advanced Ceramics A S T M C1274 Catalysts, Catalyst Supports ASTM D4567 General ISO 9277 Pharma (Active Pharmaceutical Ingredients (API) and Excipients) USP <846> Method I, European Pharmacopoeia 2.9.26 Method I a Note : Carbon Black Total (BET) and external (STSA) Surface Area evaluated by ASTM D6556 can also be determined by the AutoFlow BET+ ‘s Dynamic Flow Method and can yield equivalent results in extremely short analysis times. Table 1. Selected Examples of Dynamic Flow Test Methods for Various Materials. Figure 3. Control Module and Analysis Station Features. Touchscreen Heating Mantle Cool-down Slot Station Fittings Sample Cell Cryogen Dewar Automated Lift • • • • • • • AutoFlow BET+ surface area analyzer 5 FloWin Software Designed to maximize operator convenience with simple pre-set or user-defined measurement protocols and speedy analysis startup. FloWin software features real time displays and continuous updates of surface area measurements. Both automated and manual control of all system functions are available. Displays calculations in both graphical and tabular forms include isotherms, single- and multi-point BET analyses, t-Plot analyses with user-selectable or user-definable t-curve, all with standard or user-definable data reduction parameters and editable analysis tags. Reports are automatically generated and can be customized to seamlessly blend with your lab operations. Figure 4. FloWin Software Features. Main Menu Degas Widget Station Widget Floating Menu Figure 5. Extremely Fast Multi-Point BET Surface Area Analyses. Data Acquisition and Reduction Figure 6. Automated and Customizable Analysis Reports. AutoFlow BET+ surface area analyzer 6 Specifications - Physical FeaturesDescription1 Module2 Modules 3 Modules Sample Analysis No. of Analysis Stations 1 23 Pre-Programmed Analysis Setups Ye s User-Programmable Analyses Ye s Sample Preparation No. of Preparation Stations 333 User-Programmable Target Temp./ Ramp Rate/Soak Time Steps Up to 6 Steps per Station (18 Total) User-Adjustable Degas Flow Rates Ye s Built-In Fast-Cooling Slots Ye s Maximum Degassing Temperature 350 oC (450 oC Optional) Maximum Heating Rate 80 oC/min Degas Time Range 0-500 hours Analysis System TCD Sensors 123 Mass Flow Controllers 246 Pressure Transducers 1 Handles Pure Gases Ye s Handles Gas Mixture Inputs Ye s Automatic Multi-Path Selection Ye s Time-Saving Precalibrated Responses Ye s Manual Mode Operation Ye s Dimensions (Including CPU) Height 62 .23 cm (24.5 in) Depth 54.79 cm (21.57 in) Width 41.38 cm (16.29 in) 60 cm (23.62 in) 77.8 cm (30.63 in) Weight 34.1 kg (75 lb) 54.5 kg (111 lb) 68.8 kg (147 lb) Electrical Voltage 100-200 VAC or 220-240 VAC Frequency 50/60 Hz Power (max.) 350 VA AutoFlow BET+ surface area analyzer 7 Specifications - Technical FeaturesDescription 1 Module2 Modules 3 Modules Surface Area Single Point BET Ye s Multi-point BET Ye s Accuracy (vs. Reference Standard) ± 3.0% Repeatability (Same Station) ± 1.0% Reproducibility (Among Stations) ± 3.0% Range Limits [m 2/g] 0.01 to >3,000 Range Limits [m 2] (with N 2/77 K) 1 to 150 Analysis Speed Avg. Run Time per Sample (1-Pt. BET ) < 5 minutes< 3 minutes< 2 minutes Avg. Run Time per Sample (3-Pt. BET ) < 15 minutes< 8 minutes< 5 minutes Max. Analyses per Hour (1-Pt. BET ) 122436 Max. Analyses per Hour (3-Pt. BET ) 4812 Other Parameters Statistical Thickness Area (STSA) Ye s Micropore Surface Area (t-method) Ye s Micropore Volume (t-method) Ye s Data Reduction Automated Reporting Ye s Dedicated FloWin Software Ye s Multiple Language Options Ye s Ethernet and Remote Access Ye s User-Selectable Data Tagging Ye s Touchscreen-Accessible Functions Ye s Supports 21 CFR Part 11 Compliance Ye s AutoFlow BET+ surface area analyzer Field Service Our global service staff assure you that Quantachrome Instruments will continue to be the reliable engines of material characterization laboratories. We offer you the flexibility of choosing from service contracts tailored to provide you with the response time, service package, and spare parts discounts that best fit your needs. Spare Parts Quantachrome spare parts are certified to work with our instruments. We provide rapid response spare parts orders, and keep large inventories of replacement parts and hardware available. Application Lab Our fully equipped, state-of-the-art powder characterization laboratory (email: application-sp@anton-paar.com), provides the option of contracting for expert testing services. Laboratory services are also available to validate the applicability of our products prior to your purchase using your actual samples. Lifetime Application Support We view the field support of our instruments as an essential component of our business strategy. Our expert scientists are always available to answer questions on applications, or the use of our instruments. We do this as a standard service regardless of whether you have a service contract with us or not. Partners in Science Quantachrome has a scientific research department consisting of world renowned experts in material characterization. Our team conducts collaborative research projects with leading material research labs around the world. They regularly publish articles in leading peer reviewed journals, and speak at technical symposiums around the world. For almost half a century Quantachrome’s scientists and engineers have revolution- ized measurement techniques and designed instrumentation to enable the accurate, precise, and reliable characteri- zation of powdered and porous materials. We have an unwavering commitment to providing state of the art technology, along with superior and unparalleled customer service and support. Our commitment to customers is to support you before, during, and after the sale throughout the lifetime of our instruments. This is a big commitment because our products are so robust and reliable that we regularly find many still in use for decades. Corporate Headquarters-USA Quantachrome Instruments a brand of Anton-Paar 1900 Corporate Drive Boynton Beach, FL 33426 www.quantachrome.com Our policy of continuous development may cause the information and specifications contained herein to change without notice or liability.Trademarks and registered trade mark are the property of their respective owners. Serving Porous Materials and Powder Characterization Needs Since 1968 The quality of Quantachrome’s after sales service support is the reason we are proud to maintain life time relationships with our customers. Renowned innovator for today’s porous materials community. \251 2019 Quantachrome Corporation I06IP001EN-C