UNICUBE trace

® Combustion analysis has never been easier High data qualityFlexibilitySilent operation Ease of use N2 CO 2 H2OSO 2 KEY FEATURES • Large dynamic measurement range from 0.1 milligram chemical substance to 1 gram inhomogeneous soil • Best analysis results for any sample matrix • Wide variety of optional configurations, individually extendible • Low and tool-free maintenance • Low noise level • Low total cost of ownership • Integrated 120 position autosampler as standard • Patented ball valve for blank-free sample transfer Elemental analysis is working for you Functional principle of UNICUBE COMBUSTION GAS SEPARATION direct TPD * Trapping Column DETECTION \fample Carousel TCD Blank\bfree Ball Valv\me Combustion Tube Reduction Tube FURNACE ** The sharpest peaks in the market * Temperature Programmed Desorption ** Thermoconductivity Detector UNICUBE combines the low costs and the sensitivity of a micro elemental analyzer with the Nexibility and outstanding robustness of a macro analyzer. UNICUBE utilizes Elementar's proprietary and improved direct Temperature Programmed Desorption (direct TPD) technology for highest reliability and performance in gas separation. In combination with the most powerful detector in the market, the instrument is capable of determining samples with C:N and C:S elemental ratios of up to 12,000:1. HIGH-TEMPERATURE COMBUSTION All elemental analyzers from Elementar are designed for minimal sample preparation and secure, unattended 24?/?7 operation. They use the safe, simple and environmental friendly high-temperature combustion principle. The proven Elementar double furnace technology with separated combustion and reduction zone ensures longest maintenance intervals. In combination with an efficient, active oxygen dosing, it guarantees quantitative conversion of the sample to measuring gas — a prerequisite for highly precise and matrix-independent elemental analysis. DIRECT TEMPERATURE PROGRAMMED DESORPTION (DIRECT TPD) UNICUBE uses the proprietary direct TPD technology to chromatographically separate the combustion gases prior to detection in a highly sensitive thermoconductivity detector. The temperature program for the gas separation is controlled by a sensor positioned on the inside of the direct TPD column - directly in the gas stream. This setup has unique benefits such as very sharp peaks through direct control of the gas desorption temperature and guaranteed baseline separation of all gases - even for extreme elemental ratios. This makes the direct TPD technology capable of resolving C:N and C:S ratios of up to 12,000:1. The distinct peak separation assures absolutely reliable and trouble-free data acquisition. Elementar’s unique direct TPD columns are optimized to provide unmatched robustness and longevity compared to classic GC columns. * Temperature Programmed Desorption ** Thermoconductivity Detector Reliable results UNICUBE guarantees outstanding precision and accuracy through quantitative combustion via oxygen jet-injection directly into the combustion zone. This leads to matrix- independent results even for samples which are di?cult to combust. In combination with the state-of-the-art thermoconductivity detector, the instrument can provide an elemental detection limit down to < 50 ppm. Ease of use UNICUBE is optimized to simplify daily routine operation. Clearly arranged, easily accessible system components as well as a furnace that slides out minimize maintenance and maximize uptime. The tool-free clamp connection system ensures a reliably leak-tight instrument at any time. Thus, users can enjoy smooth analyses and confidence in their results. Thanks to a novel self-regulating cooling air circulation, UNICUBE becomes the quietest elemental analyzer in its class. A low noise level - not louder than falling rain - makes working with UNICUBE pleasant to your ear. Quiet operation Elementar Analysensysteme GmbH Elementar-Straße 1 · 63505 Langenselbold (Germany) Phone: +49 (0) 6184 9393-0 | info@elementar.de | www.elementar.de UNICUBE - high perfomance becomes easy-going ONE INSTRUMENT FOR MULTIPLE TASKS For the determination of very low S concentrations down to 2?ppm, UNICUBE can be equipped with an optional IR detector even in CHNS mode. Even oxygen and chlorine can be detected. All optionally available conversion kits allow upgrading UNICUBE at any time for special applications. The UNICUBE ® trace version obtains detection limits down to 10 ppm N. QUALITY YOU CAN TRUST Thanks to the outstanding robustness and longevity, all analyzers include a 10 year warranty on high temperature combustion furnace and thermoconductivity detector (TCD) cell. With the confidence that you will receive the highest level of technical support from our experienced team, Elementar provides spare parts for a minimum of 10 years after the end of production. This results in outstandingly low total cost of ownership. IDEAL SOLUTION FOR • Pharmaceutical laboratories • Chemical contract laboratories • Quality control laboratories • Academic research groups FOCUS SAMPLE TYPES • Chemicals • Pharmaceuticals • Polymers SAMPLE CARBON [%] HYDROGEN [%] NITROGEN [%] SULFUR [%] BIOTINE 49.21 ± 0.09 6.64 ± 0.01 11.49 ± 0.03 13.11 ± 0.05 MELAMINE 28.62 ± 0.02 4.75 ± 0.02 66.66 ± 0.04 - SULFANILIC ACID 41.59 ± 0.02 4.04 ± 0.01 8.12 ± 0.01 18.55 ± 0.03 BISMUTHIOL 15.93 ± 0.04 1.34 ± 0.02 18.68? ± 0.04 63.94? ± 0.09 NIST 141E ACETANILIDE 71.15 ± 0.02 6.78 ± 0.01 10.41? ± 0.02 - NIST 143D CYSTEINE 29.85 ± 0.02 5.04 ± 0.01 11.79 ± 0.01 26.7 2 ± 0.06 GRAPHENE 98.89 ± 0.09 0.185 ± 0.01 0.167 ± 0.01 0.214 ±0.01 3-FLUORO- ACETANILIDE 62.91 ± 0.10 4.64 ± 0.07 9.10 ± 0.03 - N-FLUOR O- BENZENE- SULFONIMIDE 29.76 ± 0.06 5.85 ± 0.01 1.65 ± 0.01 26.51 ± 0.02 Sample weight between 0.5–6?mg Easy, labor-saving instrument operation and sample preparation. Simplified maintenance. Greater silence in routine ope- ration thanks to reduced noise emission via self-regulating cooling air circulation. Outstanding precision and accuracy through high tem- perature combustion. Matrix- independent results. Longterm stability of calibration. Measure any sample matrix in any concentration. Wide range of optional conversion kits available for special applications. High data quality FlexibilitySilent operation Ease of use Art.-No. 05 005 392, 03?/?2018 A Elementar – your partner for elemental analysis Elementar is the world leader in high performance analysis of organic elements. Continuous innovation, creative solutions and comprehensive support form the foundation of the Elementar brand, ensuring our products continue to advance science across agriculture, chemical, environmental, energy, materials and forensics markets in more than 80 countries.